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Solvent-Free Buchwald-Hartwig Reaction of Aryl and Heteroaryl Halides with Secondary Amines

โœ Scribed by Topchiy, Maxim A.; Asachenko, Andrey F.; Nechaev, Mikhail S.


Book ID
121754170
Publisher
John Wiley and Sons
Year
2014
Tongue
English
Weight
199 KB
Volume
2014
Category
Article
ISSN
1434-193X

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The Buchwald-Hartwig amination reaction between p-bromotoluene and piperazine in the presence of the homogeneous catalytic system Pd(dba) 2 /(()-BINAP and the base NaO-t-Bu was investigated in two different classes of solvents: aprotic, nonpolar and aprotic, polar. The reaction was carried out using