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Solvent and Temperature Effects on the Reduction and Amination Reactions of Electrophiles by Lithium Dialkylaminoborohydrides

✍ Scribed by Pasumansky, Lubov; Collins, Christopher J.; Pratt, Lawrence M.; Vǎn Nguỹên, Ngân; Ramachandran, B.; Singaram, Bakthan

Book ID
121290976
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
147 KB
Volume
72
Category
Article
ISSN
0022-3263

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The Buchwald-Hartwig amination reaction between p-bromotoluene and piperazine in the presence of the homogeneous catalytic system Pd(dba) 2 /(()-BINAP and the base NaO-t-Bu was investigated in two different classes of solvents: aprotic, nonpolar and aprotic, polar. The reaction was carried out using