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Solute focusing using the solvent effect: Solute lagging

✍ Scribed by Pretorius, V. ;Phillips, C. S. G. ;Bertsch, W.

Publisher: John Wiley and Sons
Year: 1983
Tongue: English
Weight: 164 KB
Volume: 6
Category: Article
ISSN: 0935-6304
DOI: 10.1002/jhrc.1240060608

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✦ Synopsis

The columns listed in Table 2 were further crosslinked with azo-tert-butane 181, and their high efficiencies were still retained after crosslinking. These nonextractable columns have been successfully used in supercritical fluid chromatography [9].

In summary, small diameter capillary columns have been statically coated with SE-54 at elevated coating temperaturessuccessfully.

The methodshould prove equallysuccessfulforthe preparationof nonextractable, highly efficient columns coated with other stationary phases in other solvents. This should facilitate the use of small diameter capillary columns in both gas and supercritical fluid chromatography.

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