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Solid state synthesis of 2-aroylbenzo[b]furans, 1,3-thiazoles and 3-aryl-5,6-dihydroimidazo[2,1-b][1,3]thiazoles from α-tosyloxyketones using microwave irradiation †

✍ Scribed by Varma, Rajender S.; Kumar, Dalip; Liesen, Per J.

Book ID
118740825
Publisher
Royal Society of Chemistry
Year
1998
Weight
117 KB
Volume
24
Category
Article
ISSN
1472-7781

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✍ Yangmei Li; Marc Giulianotti; Richard A. Houghten 📂 Article 📅 2011 🏛 Elsevier Science 🌐 French ⚖ 259 KB

A facile approach to the synthesis of 2,3,6-trisubstituted-5,6-dihydroimidazo[2,1-b]thiazole was reported. A resin bound cyclic thiourea was formed by the treatment of a resin bound diamine with 1,1'-thiocarbonyldiimidazole, and then reacted with a α-haloketone to generate a resin bound isothiourea.