Solid State NMR of Polymers

✍ Scribed by Isao Ando and Tetsou Asakura (Eds.)

Publisher: Elsevier Science
Year: 1998
Tongue: English
Leaves: 1017
Series: Studies in Physical and Theoretical Chemistry 84
Edition: 1
Category: Library

No coin nor oath required. For personal study only.

✦ Synopsis

In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods.This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described.Features of this book:• Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field• Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists.This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.

✦ Table of Contents

Content:
Preface
Pages v-vi
Isao Ando, Tetsuo Asakura

Contributors
Pages xi-xiv

Introduction
Pages xv-xvi

Chapter 1 NMR chemical shift and electronic structure Original Research Article
Pages 1-21
Isao Ando, Naoki Asakawa, Graham A. Webb

Chapter 2 Dipolar interactions and interatomic distances Original Research Article
Pages 23-49
Akira Naito, Satoru Tuzi, Hazime Saitô

Chapter 3 NMR relaxations and dynamics Original Research Article
Pages 51-81
F. Horii

Chapter 4 Spin diffusion in solids Original Research Article
Pages 83-121
Matthias Ernst, Beat H. Meier

Chapter 5 NMR imaging and spatial information Original Research Article
Pages 123-163
B. Blümich, P. Blümler, K. Saito

Chapter 6 Multi-nuclear NMR Original Research Article
Pages 165-189

Chapter 6.2 ²H NMR Original Research Article
Pages 190-211
A.S. Ulrich, S.L. Grage

Chapter 6.3 ³H NMR Original Research Article
Pages 212-217
J.P. Bloxsidge, J.R. Jones, J.C. Russell, A.P. Sharratt, T.A. Vick, D. Zhong

Chapter 6.4 ¹⁵N NMR Original Research Article
Pages 218-235
T.A. Cross

Chapter 6.5 ¹⁷O NMR Original Research Article
Pages 236-252
S. Kuroki

Chapter 6.6 ¹⁹F NMR Original Research Article
Pages 253-266
Robin K. Harris, Gustavo A. Monti, Peter Holstein

Chapter 7 Structure and dynamics of crystalline and noncrystalline phases in polymers Original Research Article
Pages 267-305
Takeshi Yamanobe

Chapter 8 Oriented fibers and polymers Original Research Article
Pages 307-326
Tetsuo Asakura, Makoto Demura

Chapter 9 Polyethylene and paraffins Original Research Article
Pages 327-349
Takeshi Yamanobe, Hiromichi Kurosu

Chapter 10 Polymer blends and miscibility Original Research Article
Pages 351-414
Atsushi Asano, K. Takegoshi

Chapter 11 Polyolefins Original Research Article
Pages 415-444
Akira Aoki, Tetsuo Asakura

Chapter 12 Polyamides Original Research Article
Pages 445-468
Isao Ando, Tetsuo Asakura

Chapter 13 Poly(imide)s Original Research Article
Pages 469-490
Andrew K. Whittaker

Chapter 14 Poly(ethylene terephthalate) Original Research Article
Pages 491-507
Tetsuo Asakura, Takuro Ito

Chapter 15 Crosslinked polymers Original Research Article
Pages 509-588
R.V. Law, D.C. Sherrington

Chapter 16 Electrically-Conducting Polymers Original Research Article
Pages 589-611
Hiromichi Kurosu

Chapter 17 Inorganic polymers Original Research Article
Pages 613-666
Toshio Takayama

Chapter 18 Fluoropolymers Original Research Article
Pages 667-712
Robin K. Harris, Gustavo A. Monti, Peter Holstein

Chapter 19 Hydrogen-bonded polymers Original Research Article
Pages 713-736
Fumitaka Horii, Kenji Masuda

Chapter 20 Polymer gel systems Original Research Article
Pages 737-769
Hidekazu Yasunaga, Masatoshi Kobayashi, Shingo Matsukawa

Chapter 21 Biodegradable polymers Original Research Article
Pages 771-817
Yoshio Inoue

Chapter 22 Polypeptides Original Research Article
Pages 819-851
Isao Ando, Tsunenori Kameda, Naoki Asakawa

Chapter 23 Proteins Original Research Article
Pages 853-890
Tetsuo Asakura, Makoto Demura, Naoki Nishikawa, Hiroaki Yoshimizu

Chapter 24 Polysaccharides and biological systems Original Research Article
Pages 891-921
Hazime Saitô, Satoru Tuzi, Akira Naito

Chapter 25 NMR characterization of functionalized polysiloxanes Original Research Article
Pages 923-984
Gary E. Maciel

Conclusions
Page 985

Subject index
Pages 987-1000

📜 SIMILAR VOLUMES

Solid State NMR of Polymers

📁 Solid State NMR of Polymers

✍ Cecil Dybowski (auth.), Lon J. Mathias (eds.) 📂 Library 📅 1991 🏛 Springer US 🌐 English

The chapters in this collection are from papers which were presented at a symposium on solid-state NMR of polymers. A two-part program on available NMR techniques applicable to solid polymer analysis was presented at the 3rd Chemical Congress of North American held in Toronto, Ontario, June 5-10,

Solid State NMR of Polymers

📁 Solid State NMR of Polymers

✍ Isao Ando and Tetsou Asakura (Eds.) 📂 Library 📅 1998 🏛 Elsevier Science 🌐 English

Multidimensional Solid-State NMR and Pol

📁 Multidimensional Solid-State NMR and Polymers

✍ Klaus Schmidt-Rohr; Hans Wolfgang Spiess 📂 Library 📅 1994 🏛 Elsevier Science 🌐 English

NMR spectroscopy is the most valuable and versatile analytical tool in chemistry. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed infor

Solid-State NMR IV Methods and Applicati

📁 Solid-State NMR IV Methods and Applications of Solid-State NMR

✍ Andrew E. Bennett, Robert G. Griffin (auth.), Prof. Dr. Bernhard Blümich (eds.) 📂 Library 📅 1994 🏛 Springer-Verlag Berlin Heidelberg 🌐 English

Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance at NMR meetings, approaching that ofliquid state resonance. Important pr

NMR Spectroscopy of Polymers in Solution

📁 NMR Spectroscopy of Polymers in Solution and in the Solid State

✍ H. N. Cheng and Alan D. English (Eds.) 📂 Library 📅 2003 🏛 American Chemical Society 🌐 English

Solid State NMR

📁 Solid State NMR

✍ Niels Chr. Nielsen, Lasse A. Strassø, Anders B. Nielsen (auth.), Jerry C. C. Cha 📂 Library 📅 2012 🏛 Springer-Verlag Berlin Heidelberg 🌐 English

Dipolar Recoupling, by Niels Chr. Nielsen, Lasse A. Strassø and Anders B. Nielsen.-Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C. C. Chan.-Solid-State 19F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Ma