Solid-Phase Synthesis of Oligosaccharides and On-Resin Quantitative Monitoring Using Gated Decoupling 13 C NMR †
✍ Scribed by Kanemitsu, Takuya; Wong, Chi-Huey; Kanie, Osamu
- Book ID
- 126921322
- Publisher
- American Chemical Society
- Year
- 2002
- Tongue
- English
- Weight
- 190 KB
- Volume
- 124
- Category
- Article
- ISSN
- 0002-7863
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
## Abstract We show how high‐resolution magic angle‐spinning NMR spectroscopy can be used to characterize ^13^C‐labeled saccharides that have been prepared using solid‐phase synthesis techniques while they are still bound to a solid‐support resin. With the use of ^13^C‐labeled glucose as the starti
## Abstract The solid‐phase synthesis (SPS) of a structurally complex glycopeptide, using Sieber amide resin, was monitored by high resolution magic angle spinning NMR, demonstrating the further application of this technique. A synthetic peptidoglycan derivative, a precursor of a biologically activ