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Solid-phase synthesis of cyclic sulfonamides employing a ring-closing metathesis–cleavage strategy

✍ Scribed by Richard C.D Brown; José L Castro; Jean-Dominique Moriggi

Publisher: Elsevier Science
Year: 2000
Tongue: French
Weight: 188 KB
Volume: 41
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)00442-1

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✦ Synopsis

Ring-closing olefin metathesis using the Grubbs catalyst was applied to the cyclisative release of resin-bound sulfonamides. Flexible linkers apparently facilitated the cyclisation-cleavage, allowing a number of novel cyclic sulfonamides to be prepared in good yields using catalytic amounts of the Grubbs catalyst.

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