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Solid-Phase Synthesis of 5-Amino-1-(Substituted Thiocarbamoyl)pyrazole and 1,2,4-Triazole Derivatives via Dithiocarbazate Linker

✍ Scribed by Hwang, Jong Yeon; Choi, Hyung-Sub; Lee, Duck-Hyung; Yoo, Sung-eun; Gong, Young-Dae


Book ID
118257320
Publisher
American Chemical Society
Year
2005
Tongue
English
Weight
175 KB
Volume
7
Category
Article
ISSN
1520-4766

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✍ Vinay A. Sunagar; Prashant R. Latthe; Bharati V. Badami πŸ“‚ Article πŸ“… 2007 πŸ› Journal of Heterocyclic Chemistry 🌐 English βš– 568 KB

The Schiff bases 3a-h obtained from 4-amino-1,2,4-triazol-3-ones 1a-h when subjected to Japp-Klingemann reaction yielded the corresponding 3-{2-[(2-aryl-5-methyl-3H-[1,2,4]-triazol-3-one-4-yl)]-iminophenyl}-pentane-2,4-diones 4 a-h. These diones on cyclisation with N 2 H 4 yielded the title compound