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Simultaneous quantitative gas chromatographic determination of atropine and scopolamine

✍ Scribed by M. J. Solomon; F. A. Crane; B. L. Wu Chu; E. S. Mika

Publisher: John Wiley and Sons
Year: 1969
Tongue: English
Weight: 309 KB
Volume: 58
Category: Article
ISSN: 0022-3549
DOI: 10.1002/jps.2600580234

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✦ Synopsis

Atropine and scopolamine as free bases were simultaneously quantitated by GLC. Atropine and its sulfate salt produced peaks as apoatropine and atropine base. Scopolamine base produced peaks of scopolamine and a product of lower molecular weight. Linear standard curves were obtained between 0.5 and 200 mcg. for each alkaloid. Pure compounds and plant extracts were compared with the USP XVII assay for total alkaloids of belladonna.

Keyphrases 0 Atropine, scopolamine-simultaneous determination [7 TLC-identity 0 GLC-analysis

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