𝔖 Bobbio Scriptorium
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Simultaneous differential scanning calorimetry and small-angle x-ray scattering

✍ Scribed by Russell, T. P. ;Koberstein, J. T.

Book ID
105336065
Publisher
Wiley (John Wiley & Sons)
Year
1985
Tongue
English
Weight
355 KB
Volume
23
Category
Article
ISSN
0098-1273

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✦ Synopsis

Abstract

A method is described for performing simultaneous measurements of small‐angle x‐ray scattering and differential scanning calorimetry. The experiment is made possible through a combination of the high flux afforded by the storage ring at the Stanford Synchrotron Radiation Laboratory, a linear position‐sensitive detector with rapid response time, and a differential scanning calorimeter developed for optical microscopy. The feasibility of the technique is illustrated by examining the melting and crystallization of a polyethylene specimen. This example demonstrates the power of the technique and the accuracy and reliability of the scattering and thermal data.

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