Simultaneous determination of trace metals in human hair by dynamic ion-exchange chromatography
โ Scribed by A. Sturaro; G. Parvoli; L. Doretti; S. Zanchetta; G. Allegri; G. Battiston
- Publisher
- Elsevier Science
- Year
- 1993
- Tongue
- English
- Weight
- 650 KB
- Volume
- 274
- Category
- Article
- ISSN
- 0003-2670
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โฆ Synopsis
The simultaneous determmatlon of SIX metal ions (Cu*', Zn'+, N?+, Mn'+, Co'+, Pb") by usmg dynamic Ion-exchange chromatography IS proposed The method was apphed to the analysis of human hair after HNO,-HClO, digestion, with detectlon hnuts of ca 1 pg g -' for all the metals exammed, usmg Co as an Internal standard The quantltatlve data were confirmed by analysmg the same hair samples by atonuc absorption spectrometxy and x-ray fluorescence spectrometIy
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A method for the determmatlon of trace levels of transItion metal 1011s such as Fez+, Mn'+ and Zn2+ by hquld chromatography usmg reversed-phase Ion-pair separation, post-columu denva&atlon urlth 4\_(2-pyrldylazo)resorcmol and spectrophotometnc detection at 520 and 540 nm IS described Even tugh level