In this article, we describe an automated flow-injection system for simultaneous determination of Cl מ and total Fe. Chloride was potentiometrically determined, and total Fe was colorimetrically determined after reduction of Fe(III) to Fe(II) and complexation with 1,10-phenanthroline. Both measure
Simultaneous determination of total calcium and phosphorus in milk using flow-injection analysis
✍ Scribed by Telis Dimitrakopoulos; John R. Farrell; Peter J. Iles
- Publisher
- John Wiley and Sons
- Year
- 1998
- Tongue
- English
- Weight
- 143 KB
- Volume
- 10
- Category
- Article
- ISSN
- 0895-7533
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✦ Synopsis
The design, development, and testing of a flow-injection analysis (FIA) manifold for the simultaneous determination of two species in milk samples is reported. Calcium is determined potentiometrically, and, following on-line sample treatment, spectrophotometric analysis of phosphorus is performed. Results obtained are consistent with manufacturers' estimates and, in the case of calcium, with atomic spectrophotometric measurements. The combination FIA system is a rapid, low-cost, highly reproducible method that uses small sample volumes and could be used to provide on-site near-real-time measurements.
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