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Simultaneous determination of diclofenac sodium and its hydroxy metabolites by capillary column gas chromatography with electron-capture detection

✍ Scribed by W. Schneider; P.H. Degen

Book ID
108334862
Publisher
Elsevier Science
Year
1981
Tongue
English
Weight
444 KB
Volume
217
Category
Article
ISSN
1873-3778

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## Abstract A sensitive GC‐ECD assay has been developed for the simultaneous determination of midazolam (I) and its α‐hydroxy metabolite (II) in plasma. The assay involves extraction of both compounds into ether at alkaline pH (pH 12), followed by silylation of the α‐hydroxy metabolite with N,O‐bis