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Simultaneous CT-13C and VT-15N chemical shift labelling: Application to 3D NOESY-CH3NH and 3D 13C,15N HSQC-NOESY-CH3NH

✍ Scribed by Dušan Uhrín; Janice Bramham; Steven J. Winder; Paul N. Barlow


Book ID
111564765
Publisher
Springer Netherlands
Year
2000
Tongue
English
Weight
101 KB
Volume
18
Category
Article
ISSN
0925-2738

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✍ Weixing Zhang; William H. Gmeiner 📂 Article 📅 1996 🏛 Springer Netherlands 🌐 English ⚖ 223 KB

A 3D NOESY-(HCACO)NH experiment is described that transfers NOEs from 1H alpha to the backbone 1Hn in the succeeding residue for detection. Using this strategy, NOEs involving 1H alpha protons that resonate exactly at the water frequency can be detected. NOEs from an overlapping 1H alpha proton that