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Simple synthesis of 4-hydroxycyclohexanone

โœ Scribed by Radlick, Phillip.; Crawford, Herschel T.

Book ID
120523726
Publisher
American Chemical Society
Year
1972
Tongue
English
Weight
163 KB
Volume
37
Category
Article
ISSN
0022-3263

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Stereoselective Synthesis of ฮฒ-Hydroxycyclohexanones. -A stereoselective route to ฮฒ-hydroxycyclohexanones is reported. Thus Takai alkylidenation of the aldol (I) followed by desilylation and a novel anionic oxy-Cope rearrangement provides an enolate which undergoes 6-(enolendo)-exo-trig cyclization