The high resolution transmission electron microscope (HRTEM) imaging of short range order (SRO) in Ni 4 Mo was investigated by means of multi-slice image simulations. The HRTEM images of Ni 4 Mo exhibit locally bright dot patterns corresponding to the [001] projections of the N 2 M 2 -type (chalcopy
Short range order in Ni4Mo and its high resolution electron microscope images
β Scribed by S Hata; S Matsumura; N Kuwano; K Oki; D Shindo
- Publisher
- Elsevier Science
- Year
- 1998
- Tongue
- English
- Weight
- 857 KB
- Volume
- 46
- Category
- Article
- ISSN
- 1359-6454
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β¦ Synopsis
AbstractΓThe short range ordered (SRO) structure in Ni 4 Mo has been investigated by means of high resolution transmission electron microscopy with digital image processing and Monte Carlo simulation. High resolution transmission electron microscope (HRTEM) images were recorded with an Imaging Plate (IP) system. Conventionally printed images of the SRO state exhibit locally dot patterns corresponding to N 2 M 2 -type (chalcopyrite-like) structure. However, the dot patterns transform into those of subunit cell clusters of D1 a , D0 22 and Pt 2 Mo structures, when the image is output with a dierent gray scale. The Monte Carlo simulation with appropriate interaction parameters of atoms has explained successfully the HRTEM images. It is concluded that the SRO state in Ni 4 Mo involves subunit cell clusters of D1 a , D0 22 and Pt 2 Mo structures in the atomistic level of microstructure. The concept of h1 1/2 0i* static concentration waves corresponding to the N 2 M 2 pattern is rationalized as a mesoscopically averaging view of the SRO state.
π SIMILAR VOLUMES
in rewed form I5 Srptrmher 19753 .+bstract-The state of order of a quenched alloy of Ni,Mo was examined by making a systemanc study of electron diffraction patterns taken at a number of poles. These were of both high and low order. chosen to give a full three-dimensional description of the reciproca
The body centered cubic (a& &4.26 A s s ) -type solid solution (ss ) phase (1Ψx)Bi 2 O 3 β’ xCaO (& &0.50 < x <& &0.60 at & &820°°C) was investigated by electron diffraction. Instead of finding evidence for additional Bragg reflections at G$ $a\* as previously assumed attempting to interpret powder n