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Sequence dependence in the formation of pyroglutamyl peptides in solid phase peptide synthesis

โœ Scribed by ORLOWSKA, ALICJA ;WITKOWSKA, EWA ;IZDEBSKI, JAN

Book ID
115098660
Publisher
Wiley (Blackwell Publishing)
Year
2009
Tongue
English
Weight
258 KB
Volume
30
Category
Article
ISSN
0367-8377

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We have examined the sequence dependence of aspartimide formation during Fmoc-based solid-phase synthesis of the peptide Val-Lys-Asp-X-Tyr-Ile. The extent of aspartimide formation and subsequent conversion to the c~or [3-piperidide was characterized and quantitated by analytical reversed-phase high-