A rapid procedure utilizing high-performance liquid chromatography was developed for the separation of homooligomers of sialic acid (N-acetylneuraminic acid). The method utilizes the anion exchanger Mono-Q HR 5/S and can resolve sialyl oligomers with degrees of polymerization (DP) from 2 to 20 in 25
Separation of polyester oligomers by gradient high-performance liquid chromatography
β Scribed by Klaus Rissler
- Book ID
- 108341124
- Publisher
- Elsevier Science
- Year
- 1997
- Tongue
- English
- Weight
- 787 KB
- Volume
- 786
- Category
- Article
- ISSN
- 1873-3778
No coin nor oath required. For personal study only.
π SIMILAR VOLUMES
High-performance micro packed fused-silica and open-tubular glass capillary columns were prepared and applied to separations of complex mixtures. Solvent-gradient elution proved quite useful for the separation of solutes with wide polarity. Instruments and some applications are described. MS
## Abstract A method is presented for separation of tryptic glycopeptidesβcontaining oligosaccharides of the Nβasparagineβlinked type. High performance liquid Chromatography (HPLC) of glycopeptides on a C18 reverseβphase system eluted with a gradient of 0%β50% acetonitrile in 0.1 M NaPO~4~ pH 2.2 r