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Separation of long-chain fatty acids as phenacyl esters by high-pressure liquid chromatography

โœ Scribed by Borch, Richard F.

Book ID
120599038
Publisher
American Chemical Society
Year
1975
Tongue
English
Weight
339 KB
Volume
47
Category
Article
ISSN
0003-2700

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Separation of bile acids as their phenac
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Bile acids have been separated by high-pressure liquid chromatography. The free acids were derivatized to their phenacyl esters by treatment with triethylamine and a-bromoacetophenone. The stationary phase was a C,,, Partisil ODS column. A dual-solvent, stepwise gradient system was used for the mobi