Separation of conjugated methyl octadecadienoate and trienoate geometric isomers by silver-resin column and preparative gas-liquid chromatography
β Scribed by E. A. Emken; C. R. Scholfield; V. L. Davison; E. N. Frankel
- Book ID
- 112820346
- Publisher
- Springer-Verlag
- Year
- 1967
- Tongue
- English
- Weight
- 338 KB
- Volume
- 44
- Category
- Article
- ISSN
- 0003-021X
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A commercial mixture of conjugated linoleic acid (CLA) isomers, reportedly consisting of six components, was recently resolved into 12 peaks attributed to CLA isomers using silver-ion high performance liquid chromatography (Ag + -HPLC). In this study, the coupling of two analytical silver-ion high p
## Abstract A method has been developed for separation of linolenic acid and its seven isomers by HPLC on a silverβionβloaded column. The standard 18:3 isomers, isolated from a heated linseed oil or prepared by isomerization of linolenic acid, were converted into phenacyl esters and detected by UV