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Separation of C60 and C70 on polystyrene gel with toluene as mobile phase

✍ Scribed by Andreas Gügel; Klaus Müllen

Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
550 KB
Volume
628
Category
Article
ISSN
1873-3778

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✍ Dipl.-Chem. Andreas Gügel; Dipl.-Chem. Michael Becker; Dipl.-Chem. Dirk Hammel; 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 228 KB

Five grams of a mixture of C~60~/C~70~ can be separated in 24 hours by gel permeation chromatography on polystyrene gel. The mobile phase can be completely recovered, and the method can be scaled up by a simple increase in the inner diameter of the column.

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## Abstract Chromatographic separation of C~60~ and C~70~ fullerenes was performed with phenylpropyl and three different methoxyphenylpropyl bonded phases in microcolumn liquid chromatography. The results indicate that the 3,4‐dimethoxyphenylpropyl phase possesses the best resolving power among the