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Separation and identification of primary and secondary aliphatic amines as p-(N,N-dimethylamino)-benzene-p′-azobenzamides by paper and thin-layer chromatography

✍ Scribed by J. Churáček; H. Pechová; D. Tocksteinová; Z. żíková


Publisher
Elsevier Science
Year
1972
Tongue
English
Weight
736 KB
Volume
72
Category
Article
ISSN
1873-3778

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✍ J. Churáček; M. Hušková; H. Pechová; J. Říha 📂 Article 📅 1970 🏛 Elsevier Science 🌐 English ⚖ 676 KB

Crystalline esters cf alcol~& were prepared by means of N,N-dimethyl-$-aminobenzeneazobenzoyl chloride as reagent, and suitable conditions were found for the separation of these esters by means of paper ancl thin-layer chromatography. A detection reagent can be dispensed with as N,N-dimethyl-p-amin