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Separation and analysis of ethylenediamines as their tert.-butyldimethylsily derivatives by gas—liquid chromatography and mass spectrometry

✍ Scribed by Lay-Keow Ng


Book ID
104146692
Publisher
Elsevier Science
Year
1984
Tongue
English
Weight
376 KB
Volume
314
Category
Article
ISSN
1873-3778

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Analysis of all protein amino acids as t
✍ Chin-Joo Goh; Kenneth G. Craven; James R. Lepock; Erwin B. Dumbroff 📂 Article 📅 1987 🏛 Elsevier Science 🌐 English ⚖ 491 KB

A gas chromatographic method for the separation and quantitation of the 20 protein amino acids is described using N-methyl-N(tert.-butyldimethylsilyl)trinuoroacetamide, with 1% tert.butyldimethylchlorosilane as catalyst, to prepare the tert.-butyldimethylsilyl amino acid derivatives. Alkylsilylation