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Semiquantitative 31P-31P Homonuclear 2D J-resolved spectroscopy: Applications to oligophosphates

โœ Scribed by Janice K Gard; David R Gard


Book ID
107798575
Publisher
Elsevier Science
Year
1992
Weight
313 KB
Volume
97
Category
Article
ISSN
0022-2364

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Assignment of all 31P resonances of a 16 base-pair DNA duplex, Sd(CTGCTCACTTTCCAGG)Y Sd(CCTGGAAAGTGAGCAG)Y, related to the DNA KB site of the HIV-1 LTR, was determined by 2D heteronuclear inverse NMR spectroscopy (HSQC-TOCSY and heteronuclear COSY). 'J(H3'-P) coupling constants for most of the oligo