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Self-propagating high-temperature synthesis of SrTiO3and SrxBayTiO3(x+y=1)

✍ Scribed by A. V. Komarov; I. P. Parkin; M. Odlyha

Book ID: 104737721
Publisher: Springer
Year: 1996
Tongue: English
Weight: 816 KB
Volume: 31
Category: Article
ISSN: 0022-2461
DOI: 10.1007/bf00355902

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✦ Synopsis

Thermal initiation of mixed powders of Sr02 and titanium and/or TiE (E=02, CI3) induces a self-propagating reaction. Trituration of the product with water yielded fine crystalline particles of cubic SrTi03. Stepwise replacement of Sr02 with Ba02 in the reaction mixture generates a solid solution SrxBayTi03 (x+ y= 1). Products were characterized by X-ray powder diffraction, scanning electron microscopy, energy-dispersive analysis of X-rays and Fourier transform-infrared spectroscopy. Thermal studies were monitored by thermogravimetric analysis and differential scanning calorimetry measurements.

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