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Self-Assembly, Structure, and Spontaneous Resolution of a Trinuclear Triple Helix from an Oligobipyridine Ligand and NiII Ions

✍ Scribed by Dr. Roland Krämer; Prof. Dr. Jean-Marie Lehn; Dr. André De Cian; Prof. Dr. Jean Fischer

Publisher: John Wiley and Sons
Year: 1993
Tongue: English
Weight: 784 KB
Volume: 32
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.199307031

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## Abstract 1,3‐Bis(5′‐methyl‐2,2′‐bipyrid‐5‐yl)propane (3) can be synthesized by a two‐step procedure starting from 3‐picoline (1). In a spontaneous self‐assembly process 3 forms the binuclear triple‐stranded __meso__‐helicate [(3)~3~Fe~2~][PF~6~]~4~ on addition of iron(II) salts. The (Λ,Δ) struct