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Selenium Dioxide Insertion into the Iron-Methyl Bond of η5-C5H5Fe(CO)2CH3

✍ Scribed by Dr. Ingo-Peter Lorenz


Publisher
John Wiley and Sons
Year
1978
Tongue
English
Weight
229 KB
Volume
17
Category
Article
ISSN
0044-8249

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Synthesis and Molecular Structure of the
✍ Prof. Dr. Lothar Weber; Dipl.-Chem. Dagmar Bungardt; Uwe Sonnenberg; Dr. Roland 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 English ⚖ 389 KB 👁 1 views

40°C. Slow warm-up to room temperature, column chromatographic work-up (silica gel flash chromatography, elution with a 10 : 1 : 1 mixture of dichloromethane, petroleum ether (30-50°C) and diethyl ether), and Kugelrohr distillation (bath temperature 45 "C at 0.1 torr) afforded the a-methylene-p-lact