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Selective oxidation of organoboranes with anhydrous trimethylamine N-oxide

✍ Scribed by Soderquist, John A.; Najafi, M. Ramin


Book ID
127054154
Publisher
American Chemical Society
Year
1986
Tongue
English
Weight
992 KB
Volume
51
Category
Article
ISSN
0022-3263

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A rapid, efficient procedure for the preparation of pure, crystalline anhydrous trimethylamine N-oxide from the com.mercially available dihydrate form of the reagent is describ;d. DMF serves to both allow the distillative removal of water as well as to provide an excellent medium for obtaining large

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