Crystalline anhydrous trimethylamine N-o
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John A. Soderquist; Charles L. Anderson
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Article
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1986
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Elsevier Science
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French
β 166 KB
A rapid, efficient procedure for the preparation of pure, crystalline anhydrous trimethylamine N-oxide from the com.mercially available dihydrate form of the reagent is describ;d. DMF serves to both allow the distillative removal of water as well as to provide an excellent medium for obtaining large