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Selective One-Pot Synthesis of (Z)-Iodoallylic Iodides from Propargyl Alcohols.

โœ Scribed by Govindaswamy Manickam; Umesh Siddappa; Yong Li

Publisher
John Wiley and Sons
Year
2006
Weight
20 KB
Volume
37
Category
Article
ISSN
0931-7597

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โœฆ Synopsis

Abstract

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Efficient One-Pot Synthesis of Propargylstannanes from Propargylic Alcohol Derivatives via Allenyltitaniums. -The reaction of propargylic carbonates (I) with a Ti(OiPr) 4 /iPr-MgCl reagent combination followed by treatment with Bu 3 SnCl affords mixtures of propargylstannanes (III) and allenylstann