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Selective GLC determination of epinephrine, isoproterenol, and phenylephrine in pharmaceutical dosage forms

โœ Scribed by J. R. Watson; R. C. Lawrence


Publisher
John Wiley and Sons
Year
1977
Tongue
English
Weight
550 KB
Volume
66
Category
Article
ISSN
0022-3549

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solution of a-(carboxamidino)methanethiolsulfuric acid (1) (10.0 Gm., 0.059 mole) in 6 N hydrochloric acid (250 ml.) was heated at 96" for 17 hr. The reaction mixture was evaporated zn vacuo and the yellow gummy residue recrystallized from 50% aqueous alcohol (4.5 Gm., 550/,), m.p. 22.5-227" dec.; i