## Abstract Solid phase extraction (SPE) was evaluated as a sample pretreatment method prior to supercritical fluid extraction (SFE) of pesticides or phthalate esters from spiked water samples. ODS, Florisil, Tenax GC and XAD4 resin were evaluated for their abilities to retain a mixture of 5 pestic
✦ LIBER ✦
Selective extraction of organochlorine and organophosphorus pesticides using a combined solid phase extraction—supercritical fluid extraction approach
✍ Scribed by I.J. Barnabas; J.R. Dean; S.M. Hitchen; S.P. Owen
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 548 KB
- Volume
- 291
- Category
- Article
- ISSN
- 0003-2670
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✦ Synopsis
Supercritical fluid extraction WE) of pesticides has been investigated for the possibility of selective extraction between organochlorine (OCPs) and organophosphorus (OPPs) compounds. Three OCPs and OPPs were trapped onto a C,, EmporeTM extraction disk prior to WE with CO, only and methanol-modified CO, at various pressures and constant temperature. The results indicate that OCPs can be quantitatively extracted using CO2 only whereas OPPs require a modifier for extraction.
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