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Selective extraction of organochlorine and organophosphorus pesticides using a combined solid phase extraction—supercritical fluid extraction approach

✍ Scribed by I.J. Barnabas; J.R. Dean; S.M. Hitchen; S.P. Owen


Publisher
Elsevier Science
Year
1994
Tongue
English
Weight
548 KB
Volume
291
Category
Article
ISSN
0003-2670

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✦ Synopsis


Supercritical fluid extraction WE) of pesticides has been investigated for the possibility of selective extraction between organochlorine (OCPs) and organophosphorus (OPPs) compounds. Three OCPs and OPPs were trapped onto a C,, EmporeTM extraction disk prior to WE with CO, only and methanol-modified CO, at various pressures and constant temperature. The results indicate that OCPs can be quantitatively extracted using CO2 only whereas OPPs require a modifier for extraction.


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Supercritical fluid extraction of pestic
✍ John L. Ezzell; Bruce E. Richter 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 410 KB

## Abstract Solid phase extraction (SPE) was evaluated as a sample pretreatment method prior to supercritical fluid extraction (SFE) of pesticides or phthalate esters from spiked water samples. ODS, Florisil, Tenax GC and XAD4 resin were evaluated for their abilities to retain a mixture of 5 pestic