Selective enzymatic removal of protecting groups: The phenylacetamide as amino protecting group in phosphopeptide synthesis
โ Scribed by Herbert Waldmann; Axel Heuser; Sonja Schulze
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- French
- Weight
- 240 KB
- Volume
- 37
- Category
- Article
- ISSN
- 0040-4039
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๐ SIMILAR VOLUMES
I and I1 reacted on the carrier to form V (53% based on 11-gel polymer) and 111 and IV reacted on the carrier to give VI (24 % based on IV-gel polymer). V was again released from the carrier, purified, and combined with VI on the carrier to give the fully protected final product VII (32'x based on V
## Abstract 2โThiopyridone (2โmercaptopyridine, **1**) was found to be a very suitable reagent for removing the __N__^ฮฑ^โoโnitrophenylsulfenyl (NPSโ) group in both conventional and solidโsupport peptide synthesis. A 3โ to 5โmolar excess of the reagent together with an equivalent amount of glacial a
## Abstract For Abstract see ChemInform Abstract in Full Text.