𝔖 Bobbio Scriptorium
✦   LIBER   ✦

(S)-Methyl 2-[(furan-2-carbon­yl)amino]-3-phenyl­propanoate

✍ Scribed by Zeng, Xiang Chao ;Li, Li Hong ;Cen, Ying Zhou


Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
172 KB
Volume
62
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


The title compound, C 15 H 15 NO 4 , was synthesized by acylation of methyl l-2-amino-3-phenylpropanoate with furan-2carbonyl chloride at room temperature. In the crystal structure, intermolecular N-HÁ Á ÁO hydrogen bonds link the molecules into extended chains parallel to the b axis.


📜 SIMILAR VOLUMES


3-(5-Methyl­furan-2-yl)propanoic acid
✍ Frey, Wolfgang ;Grundl, Li ;Hashmi, A. Stephen K. 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 228 KB
Methyl 2-(4-methylphenylsulfonamido)-3-p
✍ Yin, Ping ;Hu, Mao-Lin ;Xiong, Jing ;Yan, Xiao-Wei 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 900 KB

The title compound, C 17 H 19 NO 4 S, has two independent molecules in the asymmetric unit linked by an N-HÁ Á ÁO hydrogen bond. The principal difference between them lies in the relative orientations of the two aromatic rings. These are inclined at an angle of 3.70 (3) in one molecule but at 58.41

Ethyl 2-{[(1Z)-(3-methyl-5-oxo-1-phenyl-
✍ Zhang, Xin ;Zhu, Hua-Ling ;Xu, Hai-Zhen ;Dong, Mei 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 189 KB

In the title compound, C 28 H 27 N 3 O 3 , the pyrazolone ring and the N atom of the 2-amino-3-phenylpropanoate group are essentially coplanar. The compound is in an enamine-keto form and its structure is stabilized by one strong intramolecular N-HÁ Á ÁO hydrogen bond.

Methyl 3-(2-oxobenzo­thia­zolin-3-yl)­pr
✍ Ersanlı, Cem Cüneyt ;Dündar, Yasemin ;Sarı, Ugˇur ;Noyanalpan, Ningur ;Odabaşogˇ 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 304 KB
Ethyl 3-{[(2-chloro­phenyl)­sulfonyl]­im
✍ Kennard, Colin H. L. ;McFadden, Helen G. ;Byriel, Karl A. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 314 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.010 A Ê Disorder in main residue R factor = 0.043 wR factor = 0.152 Data-to-parameter ratio = 14.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.