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(S)-(Acetyl­acetonato-κ2O,O′)[2-(1-aminoethyl)­phenyl-κ2C1,N]­palladium(II)

✍ Scribed by Calmuschi, Beatrice ;Englert, Ulli

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
212 KB
Volume
61
Category
Article
ISSN
1600-5368

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(S)-[2-(1-Amino­ethyl)­phenyl-κ2C1,N](he
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✍ Calmuschi, Beatrice ;Englert, Ulli 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 251 KB

Single-crystal X-ray study T = 110 K Mean '(C±C) = 0.007 A Ê R factor = 0.037 wR factor = 0.095 Data-to-parameter ratio = 17.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The structure of the title complex, [Ni 2 (C 5 H 7 O 2 ) 4 (H 2 O) 2 ]Á-0.5H 2 O, is dimeric and corresponds to the trimeric structure of bis(acetylacetonato)nickel(II) in which one Ni(acac) 2 unit is replaced by two water molecules. The centrosymmetric molecule comprises two O-O edge-shared octahed

(Acetyl­acetonato-κ2O,O′)(oxalato-κ2O,O′
(Acetyl­acetonato-κ2O,O′)(oxalato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)chromium(III) trihydrate
✍ Wang, Wen-Bo ;Yang, Li-Xin ;Chen, Fang-Fei 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 288 KB

The title ternary mixed-ligand chromium(III) complex, [Cr(C~5~H~7~O~2~)(C~2~O~4~)(C~12~H~8~N~2~)]·3H~2~O, features a distorted octahedral geometry completed by three different bidentate chelating ligands, __viz__. 1,10-phenanthroline, acetylacetonate and oxalate. Complex molecules are linked by π–π