Rotor design for high pressure magic angle spinning nuclear magnetic resonance
β Scribed by Romulus V.F. Turcu; David W. Hoyt; Kevin M. Rosso; Jesse A. Sears; John S. Loring; Andrew R. Felmy; Jian Zhi Hu
- Book ID
- 119300302
- Publisher
- Elsevier Science
- Year
- 2013
- Tongue
- English
- Weight
- 463 KB
- Volume
- 226
- Category
- Article
- ISSN
- 1090-7807
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## Abstract Highβresolution NMR spectra of materials subject to anisotropic broadening are usually obtained by rotating the sample about the magic angle, which is 54.7Β° to the static magnetic field. In projected magic angle spinning (pβMAS), the sample is spun about two angles, neither of which is
## Abstract The recently developed technique of gradient, highβresolution magicβangle spinning NMR (gβhrβMASβNMR) spectroscopy was applied to the study of __ex vivo__ human lipoma and liposarcoma tissue. Compared with conventional ^1^HβNMR, the gβhrβMAS method yielded a large improvement in spectra