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Ring opening of 1,2-bis(trimethylsiloxy)-1,2-dimethylcyclopropanediol with hydrogen bromide and bromine

✍ Scribed by Breitbeil, Fred W.; Schranz, John L.

Book ID: 127215099
Publisher: American Chemical Society
Year: 1979
Tongue: English
Weight: 377 KB
Volume: 44
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00393a038

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## Abstract The reactions of 1,2‐hexadecanediol and 1,2‐octadecanediol with hydrogen bromide in the presence of acetic anhydride have been investigated. The treatment of hydrogen bromide (48%) in acetic anhydride with 1,2‐hexadecanediol gives mainly 1‐bromo‐2‐acetoxy hexadecane (66%), 2‐acetoxy hex