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Regioselective Hydrazination of 6-Arylidene-2-furfurylidene-cyclohexanones: Syntheses of 3-Aryl-7-furfurylidene-3,3a,4,5,6,7-hexahydro-2H-indazoles.

✍ Scribed by A. A. Bugaev; A. G. Golikov; Yu. A. Fomina; S. V. Egorov; A. P. Kriven'ko

Publisher
John Wiley and Sons
Year
2005
Weight
15 KB
Volume
36
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

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Synthesis and 1H and 13C NMR study of the stereochemistry of (E )-2-acetyl-3-aryl-7-arylidene-3,3a,4,5,6,7-hexahydroindazoles
✍ V. Vijayabaskar; S. Perumal; S. Selvaraj; M. J. E. Hewlins πŸ“‚ Article πŸ“… 1999 πŸ› John Wiley and Sons 🌐 English βš– 113 KB πŸ‘ 2 views

The reaction of 2,6-diarylidenecyclohexanones with hydrazine hydrate in glacial acetic acid resulted in the formation of diastereomers of (E)-2-acetyl-3-aryl-7-arylidene-3,3a,4,5,6,7-hexahydroindazoles. The relative conÐgurations of these diastereomers were unambiguously assigned using 1H and 13C NM