Refinement of solid-state MAS NMR spectra of quadrupolar nuclei: Application to the analysis of some 51V compounds
✍ Scribed by P Bodart; J.P Amoureux; C Fernandez
- Book ID
- 103909871
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 186 KB
- Volume
- 12
- Category
- Article
- ISSN
- 0730-725X
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
Three population transfer techniques for improving the sensitivity of the central transition of NMR spectra from half-integer quadrupolar nuclei in the solid state are described. Two of the methods attempt to invert the populations of energy levels associated with the satellite transitions either by
## Abstract ^13^C CP/MAS NMR spectra (50.3 MHz) of 4‐[__N__,__N__‐bis(2‐hydroxyethyl)amino]azobenzene (1), (__N__,__N__‐dimethylamino)azobenzene (2), 4‐methoxyazobenzene (3), 2‐hydroxy‐5‐__tert__‐butylazobenzene (4) and 4‐hydroxyazobenzene (5) were recorded. The isotopomers of 1, 4 and 5 with penta