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Spectral Editing of Solid-State MAS NMR Spectra of Half-Integer Quadrupolar Nuclei

โœ Scribed by Caldarelli, Stefano; Ziarelli, Fabio


Book ID
125901857
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
30 KB
Volume
122
Category
Article
ISSN
0002-7863

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๐Ÿ“œ SIMILAR VOLUMES


QCPMG-MAS NMR of Half-Integer Quadrupola
โœ Flemming H. Larsen; Hans J. Jakobsen; Paul D. Ellis; Niels Chr. Nielsen ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 97 KB

By combination of fast magic-angle spinning (MAS) and detection of the free-induction decay during a rotor-synchronized quadrupolar Carr-Purcell-Meiboom-Gill (QCPMG) train of refocusing pulses, the sensitivity of quadrupolar-echo MAS NMR spectra for the central transition of half-integer quadrupolar

High-resolution multiple quantum MAS NMR
โœ Gang Wu; David Rovnyank; Boqin Sun; Robert G. Griffin ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 500 KB

We demonstrate the utility of a two-pulse sequence in obtaining high-resolution solid state NMR spectra of half-integer quadrupolar nuclei with magic-angle-spinning (MAS). The experiment, which utilizes multiple/single-quantum correlation, was first described in a different form by Frydman and Harwo