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Reductive halogenation of epoxides induced by halosilanes and 1,1,3,3-tetramethyldisiloxane (TMDS)

✍ Scribed by Jesus M. Aizpurua; Claudio Palomo

Book ID
103398773
Publisher
Elsevier Science
Year
1984
Tongue
French
Weight
97 KB
Volume
25
Category
Article
ISSN
0040-4039

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## Abstract An efficient reduction of aromatic and aliphatic esters with 1,1,3,3‐tetramethyldisiloxane in combination with [MoO~2~(acac)~2~] or [V(O)(O__i__Pr)~3~] is reported. In the former system, the presence of triphenylphosphane oxide allows high conversion and good isolated yield to be reache