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Reduction of olefins on solid support using diimide

✍ Scribed by Patrick Lacombe; Bastien Castagner; Yves Gareau; Réjean Ruel


Book ID
104259842
Publisher
Elsevier Science
Year
1998
Tongue
French
Weight
110 KB
Volume
39
Category
Article
ISSN
0040-4039

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✦ Synopsis


The reduction of solid supported olefinic substrate using diimide is described. The diimide, prepared from sulfonylhydrazide, was found to efficiently reduce the olefinic substrates. Typically, the reaction proceeds in over 90% yield to afford the reduction product cleanly after cleavage from the Wang resin.


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