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Reduction of hexachloroacetone by 1-benzyl-1,4-dihydronicotinamide

✍ Scribed by Donald C. Dittmer; Louis J. Steffa; John R. Potoski; Roger A. Fouty

Publisher: Elsevier Science
Year: 1961
Tongue: French
Weight: 138 KB
Volume: 2
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)82671-x

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✦ Synopsis

HEXACHLOROACETONE is very readily reduced to hexachloroisopropanol by I-benzyl-l,f+-dihydronicotinamide. The reduction goes violently at room and is accompanied went vigorously. temperature in the absence of solvent, is exothermic, by formation of a black tar. Even at 0' the reaction cc13cocc13 + HCl Best yields -+ (CC13)CHO-+ CON&J (CCl+CHOH +

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