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Reduction of Arylmethyl Chlorides with a Phosphine-Hydrogen Mixture in the KOH-DMSO System

✍ Scribed by S. F. Malysheva; V. A. Kuimov; B. G. Sukhov; N. K. Gusarova

Publisher
Springer
Year
2005
Tongue
English
Weight
30 KB
Volume
75
Category
Article
ISSN
1070-3632

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The reaction of red phosphorus with 1-bromonaphthalene in the KOH–DMSO system: Synthesis of tri(1-naphthyl)phosphane
✍ Vladimir A. Kuimov; Svetlana F. Malysheva; Nina K. Gusarova; Tamara I. Vakul'ska 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 English ⚖ 163 KB

## Abstract Red phosphorus reacts with 1‐bromonaphthalene in the KOH–DMSO system upon heating (47–70°C, 3 h) to give tri(1‐naphthyl)phosphane in 10% yield. Microwave activation (600 W, 6 min) of the reaction affords the above‐mentioned phosphane in 25% yield. © 2011 Wiley Periodicals, Inc. Heteroat