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Reduction of 4-Nitropyridine N-Oxide with Low Valent Titanium Reagent

✍ Scribed by Dr. Łukasz Kaczmarek; Dr. Roman Balicki; Dr. Marek Malinowski


Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
125 KB
Volume
332
Category
Article
ISSN
1615-4150

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A novel reductive cyclization of o-nitro
✍ Da-Qing Shi; Liang-Ce Rong; Ju-Xian Wang; Qi-Ya Zhuang; Shu-Jianga Tu 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 405 KB 👁 1 views

## Abstract A short and facile synthesis of a series of 1, 2‐dihydroquiazolin‐4(3H)‐ones was accomplished in good yields via novel reductive cyclization of o‐nitrobenzamides with ketones promoted by TiCl~4~/Zn system. The structure was established on the basis of elemental analysis, IR, 'H NMR and