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Facile Reductive Cleavage of Oximes with a Low-Valent Titanium Reagent

✍ Scribed by Balicki, Roman ;Kaczmarek, Lukasz ;Malinowski, Marek


Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
144 KB
Volume
1989
Category
Article
ISSN
0947-3440

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## Abstract A short and facile synthesis of a series of 1, 2‐dihydroquiazolin‐4(3H)‐ones was accomplished in good yields via novel reductive cyclization of o‐nitrobenzamides with ketones promoted by TiCl~4~/Zn system. The structure was established on the basis of elemental analysis, IR, 'H NMR and