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Reassignment of NMR spectra and conformational study of the sesquiterpene lactone goyazensolide

✍ Scribed by Katia S. P. Perry; Eduardo Miguez; Mauro B. de Amorim; Maria Amelia D. Boaventura; Antonio Jorge R. da Silva


Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
106 KB
Volume
39
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

We describe the reassignment of ^13^C NMR signals of goyazensolide based upon 1D and 2D techniques, and discuss its conformation and stereochemistry as obtained from the analysis of its proton spin–spin coupling constants, NOE measurements and molecular mechanics calculations using MM3* force field. Copyright © 2001 John Wiley & Sons, Ltd.


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