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Reaction of methanesulfinyl chloride with water

✍ Scribed by Norton, Richard V.; Beverly, Gordon M.; Douglass, Irwin B.

Book ID
126831148
Publisher
American Chemical Society
Year
1967
Tongue
English
Weight
428 KB
Volume
32
Category
Article
ISSN
0022-3263

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## Abstract A new procedure for the synthesis of methanesulfinyl chloride is described which involves chlorination of dimethyl disulfide with sulfuryl chloride in the presence of hexamethyldisiloxane. The use of ^18^O‐labelled hexamethyldisiloxane in this reaction results in the formation of ^18^O‐