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Reaction of hexamethylphosphoric triamide with alkyllithiums. In situ formation of N-methylmethylenimine

✍ Scribed by Abatjoglou, Anthony G.; Eliel, Ernest L.

Book ID
126889824
Publisher
American Chemical Society
Year
1974
Tongue
English
Weight
258 KB
Volume
39
Category
Article
ISSN
0022-3263

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Herein we report the facile conversion of 2 ,3 ,5 -tri-O-acetylinosine to three different nucleoside analogs via reaction of hexamethylphosphorous triamide and an organic halide. Acetyl-protected 6-bromopurine riboside, 6-chloropurine riboside and N 6 ,N 6 -dimethyladenosine can each be prepared in