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Reaction of chloroacetylenephosphonate with acetoacetic ester and its analogs

โœ Scribed by V. A. Khramchikhin; G. V. Yacobson; A. V. Dogadina; A. V. Khramchikhin; B. I. Ionin

Book ID
111460450
Publisher
Springer
Year
2010
Tongue
English
Weight
115 KB
Volume
80
Category
Article
ISSN
1070-3632

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Penta-O-actyl-l,2-dideoxy-l-nitro-D-gluco-hept-l-enitol reacts with methyl acetoacetate in an unusual Michael reaction, giving the normal adduct (6), and a bicyclic derivative (9) that arises from quasi-dimerization of the former when a high concentration of the base is used. Acetylation of compound