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Reaction of 4-(2′-Hydroxyaryl)-1,3-dithiolium Salts with Sodium Sulfide. A Selective Synthesis of 2′-Hydroxyacetophenones.

✍ Scribed by Mihail Lucian Birsa

Publisher
John Wiley and Sons
Year
2003
Weight
81 KB
Volume
34
Category
Article
ISSN
0931-7597

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~~~ ~ ~ ~ 4-Aryl-substituted 3,5-bis(methylthio)-1,2-dithiolium salts 9a, 10a were isolated. 4-Alkyl-substituted 1,3-bis(methylsuch as l a react with metal cyclopentadienides 4 (M+ = TI, thio)-1,2-dithiolium salts such as l c react with thallium cyclo-Li) mainly by cleavage of the S-S bond. A subseq